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| 1st(1st leg) | Espanyol Barcelona | - | FC Barcelona | 1:2 (0:2) | ||
| 2nd (2nd leg) | FC Barcelona | - | Espanyol Barcelona | 1:1 (1:1) | ||
| 1st(1st leg): 30/01/2001 20:30 | 2nd (2nd leg): 07/02/2001 20:00 | Winner: FC Barcelona | ||||
| 1st(1st leg) | Racing Santander | - | Real Zaragoza | 1:1 (0:1) | ||
| 2nd (2nd leg) | Real Zaragoza | - | Racing Santander | 2:0 (1:0) | ||
| 1st(1st leg): 31/01/2001 19:45 | 2nd (2nd leg): 07/02/2001 20:00 | Winner: Real Zaragoza | ||||
| 1st(1st leg) | RC Celta | - | RCD Mallorca | 3:1 (0:1) | ||
| 2nd (2nd leg) | RCD Mallorca | - | RC Celta | 2:1 (1:0) | ||
| 1st(1st leg): 31/01/2001 20:15 | 2nd (2nd leg): 07/02/2001 20:00 | Winner: RC Celta | ||||
| 1st(1st leg) | Granada CF | - | Atlético Madrid | 0:1 (0:1) | ||
| 2nd (2nd leg) | Atlético Madrid | - | Granada CF | 3:1 (1:0) | ||
| 1st(1st leg): 31/01/2001 20:15 | 2nd (2nd leg): 06/02/2001 20:30 | Winner: Atlético Madrid | ||||
